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ЦТМТНА.Вот проклятье!!!(+)
exploders.info - Портал по взрывчатым веществам и пиротехнике
АВТОРИЗАЦИЯ
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Автор:
[#16094]

ЦТМТНА.Вот проклятье!!!(+)

Форум: Индивидуальные ВВ

Что за черт.Ну не получаются у меня нормальные ВВ.Я наверное уже всем надоел со своими неудачами.Тут уж народ на всякие HNIWы,NTO и DINGU перешел а у меня и такая фигня как ЦТМТНА не получается. Может у меня руки кривые? Сейчас пробовал варить ЦТМТНА(а как кто-то уже говорил вернее морозить).Перечитал кучу советов и рецептов и решил делать так: В 0.5 литр. банку налил 32мл эл-та, добавил примерно такое же по объему кол-во льда.Подождал пока t° не опустится до 0°С и вылил туда охлажд. до 5°С р-р 8г уротропина в 40мл воды.Подождал пока смесь снова охладится до 0 и разом прилил р-р 20г NaNO2 в 40мл воды. Все пишут что сразу должна начаться бурная реакция и появиться много желтой пены.У меня же смесь просто немного вспенилась(t° держалась 5-6°С), через несколько сек. пена исчезла и ничего, больше так ничего и не появилось.Попробовал добавить чуток нитрита, опять вспенилось на несколько сек. и все. Воняло немного NO2, формальдегидом по моему нифига. NaNO2 делал восстановлением нитрата мелкими кусочками свинца варил 2ч,получил белый порошок отличающийся от нитрата негигроскопичностью.Думал может нитрит не получился и потом сыпанул в банку щепотку NaNO3- на нее вообще нет реакции.Значит у меня NaNO2 был!

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